MC: Premier Materials Characterization Methods- is written in order to use it as lecture notes for TECHNIQUES OF MATERIALS CHARACTERISATION and it can also be used as textbook. This book FIVE CHAPTERS, viz., Chapter I - THERMAL ANALYSIS, Chapter II - OPTICAL MICROSCOPY, Chapter III - ELECTRON MICROSCOPY, Chapter IV - ELECTRICAL METHODS and Chapter V - SPECTROSCOPIC ANALYSIS. This book contains 100% lecture notes to explain MATERIALS CHARACTERISATION TECHNIQUES. This book style is lucid and contains 100% notes to explain briefly. Though descriptive theories are not presented, this book covers cent per cent examination stuffs for M.E.(Cryogenic Engineering) and Ph.D.(Physical Sciences).