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Material Characterization Tests: For Objects of Art and Archaeology

Autor Nancy Odegaard, Scott Carroll, Werner S. Zimmt
en Limba Engleză Paperback – 9 iul 2015
The first edition of this book was welcomed not only by the conservation profession but also by those working in archaeology and museums who need to know from what materials objects are made, the compounds that are associated with them or the characteristics of the materials used to package or store them. This second edition (reprint) includes modifications to several of the procedures described - tests for metals, inorganic compounds, organic and synthetic materials as well as several tests that help to characterize materials. The tests are applicable to a wide range of object classes including metal, textile, leather, paper, plastics and architectural materials. In addition to presenting the detailed methodology for carrying out each test, the authors have evaluated the effectiveness of each test in order to assist the reader in selecting the most applicable test and interpreting the results.
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Specificații

ISBN-13: 9781909492202
ISBN-10: 1909492205
Pagini: 242
Greutate: 0.73 kg
Ediția:Revised
Editura: Archetype Publications

Descriere

The first edition of this book was welcomed not only by the conservation profession but also by those working in archaeology and museums who need to know from what materials objects are made, the compounds that are associated with them or the characteristics of the materials used to package or store them. This second edition (reprint) includes modifications to several of the procedures described - tests for metals, inorganic compounds, organic and synthetic materials as well as several tests that help to characterize materials. The tests are applicable to a wide range of object classes including metal, textile, leather, paper, plastics and architectural materials. In addition to presenting the detailed methodology for carrying out each test, the authors have evaluated the effectiveness of each test in order to assist the reader in selecting the most applicable test and interpreting the results.


Cuprins

Foreword for UK readers

Acknowledgements


Introduction


Chemical safety


Scientific method and techniques of spot testing


Spot tests for metals

Test for aluminium ions using aluminon (aurintricarboxylic acid)

Test for aluminium metal using Alizarin Red S and electrolysis

Test for antimony using spot-test papers

Test for arsenic compounds using spot-test papers

Test for arsenic or phosphorus in copper metal using iron(III) chloride

Test for chromium using diphenylcarbazide and electrolysis

Test for copper using spot-test papers

Test for copper using nitric acid and ammonia

Test for copper using potassium ferrocyanide

Test for copper using rubeanic acid

Test to determinate gold karat using a touchstone

Test to determinate gold quality using nitric acid

Test for gold using tin (II) chloride and electrolysis

Test for gold plating using aqua regia

Test for iron using potassium ferrocyanide

Test for iron using hydrochloric acid

Test for lead using spot-test papers

Test for lead using potassium iodide and electrolysis

Test for lead using potassium dichromate

Test for mercury salts using diphenylcarbazone

Test for mercury using aqua regia

Test for mercury-cinnabar using a melting point apparatus

Test for nickel using spot-test papers

Test for nickel using dimethylglyoxime

Test for silver using potassium dichromate

Test for silver using potassium dichromate and electrolysis

Test to determine silver quality using nitric acid

Test for tin using cacotheline using electrolysis

Test for tin using sulfurous acid

Test for zinc using ammonium mercuric thiocyanate

Test for zinc in copper alloy using electrolysis

Test for zinc using spot-test papers


Spot tests for inorganic and ionic materials

Test for calcium using nitric acid and sulfuric acid

Test for carbonate using hydrochloric acid and barium hydroxide

Test for chloride ions using sulfuric acid

Test for halogens (chlorine) using pyrolysis (Beilstein test)

Test for chloride using silver nitrate

Test for chlorine in polymers using pH paper and pyrolysis

Test for nitrate using spot-test papers

Test for nitrate using iron(II) sulfate

Test for phosphate using spot-test papers

Test for phosphate using ammonium molybdate and benzidine

Test for phosphate using ammonium molybdate and ascorbic acid

Test for sulfate using spot-test papers

Test for sulfate using barium chloride


Spot tests for organic materials

Test for starch using iodine/potassium iodide

Test for simple carbohydrates using o-toluidine

Test for complex carbohydrates using o-toluidine

Test for carbohydrates using triphenyltetrazolium chloride

Test for triglycerides using triglyceride reagent

Test for unsaturated oils using potassium permanganate

Test for blood using benzidine

Test for protein (nitrogen) using calcium oxide and pyrolysis

Test for protein using copper(II) sulfate (Biuret test)

Test for sulfur using lead acetate paper and pyrolysis

Test for organic sulfur using calcium oxalate and pyrolysis

Test for phenols in vegetable-tanned leather using lead acetate

Test to determine vegetable-tanned leather using iron(III) sulfate

Test for indigo using sodium hydrogen sulfite

Test for lignin using phloroglucinol

Test for rosin using sulfuric acid (Raspail test)

Test for cellulose using aniline acetate and pyrolysis

Test for cellulose and its derivatives using 1-naphthol (Molisch test)

Test for nitrate (cellulose nitrate) using diphenylamine

Test for poly(vinyl alcohol) using iodine/potassium iodide

Test for polyester groups using hydroxylamine hydrochloride

Test for polyamides using p-dimethylaminobenzaldehyde

Test for polycarbonates using p-dimethylaminobenzaldehyde

Test for silicone-based rubber using pyrolysis


Other tests

Test of pH using an Insta-Check(R) pH pencil

Test for acidity with pH pens

Test for volatile acids with pH papers and lime water

Test for volatile acides with pH papers and glycerol

Test for acidic vapors using cresol red

Test for hardness with a pencil sequence

Test to determine specific gravity using an electronic analytical balance

Test for radioactivity using photographic film


Appendix 1: Dilution table and chemical concentration calculations

Appendix 2: Explanation of pH

Appendix 3: List of abbreviations

Appendix 4: Table of reagents with safety information used in spot tests

Appendix 5: Chemicals, equipment and supplies

Appendix 6: Product suppliers

Appendix 7: Materials Characterization Trial Form

Appendix 8: Glossary

Appendix 9: Bibliography

The first edition of this book was welcomed not only by the conservation profession but also by those working in archaeology and museums who need to know from what materials objects are made, the compounds that are associated with them or the characteristics of the materials used to package or store them.