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Modern NMR Approaches to the Structure Elucidation of Natural Products: Data Acquisition and Applications to Compound Classes de Antony Williams

Modern NMR Approaches to the Structure Elucidation of Natural Products: Data Acquisition and Applications to Compound Classes: Modern NMR Approaches to Natural Products Structure Elucidation

Editat de Antony Williams, Gary Martin, David Rovnyak
en Limba Engleză Hardback – 25 sep 2016
This book is part of a two-volume set regarding the structure elucidation of natural products. Book 1 will discuss contemporary NMR approaches. It will cover optimized hardware and experimental approaches to obtain both the highest quality and most appropriate spectral data for analysis. It will also discuss data processing and algorithmic based analysis of the data to extract molecular structures. This meshing of details regarding data acquisition, software and hardware approaches to the elucidation of natural products will bring together a selection of experts in the field and will be the first monograph of its kind. Book 2 will review the application of NMR to the analysis of a series of different natural product families including marine natural products, anti-cancer agents, alkaloids, terpenes, steroids, antibiotics, terpenes, carbohydrates, peptides and venoms. There are no books on the market that are focused on the unique combination of experimental approaches and modern hardware and software approaches to the structure elucidation of natural products. These books will, over 2 volumes, bring together acknowledged experts in the field of natural products structure elucidation. These volumes will be attractive to the readers as the series will offer a unique and much-needed perspective of contemporary approaches.
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Specificații

ISBN-13: 9781849733939
ISBN-10: 1849733937
Pagini: 304
Dimensiuni: 156 x 234 x 36 mm
Greutate: 0.91 kg
Editura: Royal Society Of Chemistry
Seria Modern NMR Approaches to Natural Products Structure Elucidation

Textul de pe ultima copertă

The Ghanian plant Cryptolepis sanguinolenta is the source of a series of fascinating indoloquinoline alkaloids. The most unusual member of this alkaloid series was initially proposed to be a spiro nonacyclic structure, named cryptospirolepine, and was elucidated in 1993 based on the technologies available at that time. There were, however, several annoying attributes to the structure that bothered analysts for the ensuing 22 years. During the two decades that followed the initial work there have been enormous developments in NMR technology. Using new experimental approaches, specifically homodecoupled 1,1- and 1, n-HD-ADEQUATE NMR experiments developed in 2014, the structure of only a 700 ug sample of cryptospirolepine has been revised and is shown on the cover of this volume. The confluence of the NMR technological and methodological advances that allowed the revision of the structure of cryptospirolepine using a submilligram sample seems a fitting example for this book, which is dedicated to the NMR characterization of various classes of natural products.

Volume 2 considers data processing and algorithmic based analyses tailored to natural product structure elucidation and reviews the application of NMR to the analysis of a series of different natural product families including marine natural products, terpenes, steroids, alkaloids and carbohydrates. Volume 1 discusses contemporary NMR approaches including optimized and future hardware and experimental approaches to obtain both the highest quality and most appropriate spectral data for analysis. These books, bringing together acknowledged experts, uniquely focus on the combination of experimental approaches and modern hardware and software applied to the structure elucidation of natural products. The volumes will be an essential resource for NMR spectroscopists, natural product chemists and industrial researchers working on natural product analysis or the characterization of impurities and degradation products of pharmaceuticals that can be as scarce as natural product samples."