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Techniques and Experiments for Organic Chemistry

Autor Addison Ault
en Limba Engleză Hardback – 31 ian 1998
This student text explains how to perform operations, as well as providing recipes for the preparation of a variety of organic compounds. There are sections on procedures, techniques, safety, glassware, clean up, collection and disposal of waste, and the laboratory notebook.
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Specificații

ISBN-13: 9780935702767
ISBN-10: 0935702768
Pagini: 664
Ilustrații: illustrations
Dimensiuni: 198 x 242 x 36 mm
Greutate: 1.34 kg
Ediția:Revizuită
Editura: University Science Books
Locul publicării:Sausalito, United States

Cuprins

Safety
Glassware Used in the Organic Chemistry Lab
Cleaning Up
Collection and Disposal of Waste
The Laboratory Notebook
The Chemical Literature
Tables
Filtration
Recrystallization
Distillation
Reduced-Pressure Distillation
Distillation of Mixtures of Two Immiscible Liquids: Steam Distillation
Sublimation
Extraction by Solvents
Chromatography
Removal of Water
Boiling Point
Melting Point
Density
Index of Refraction
Optical Activity
Molecular Weight
Solubility
Infrared Absorption Spectrometry
Ultraviolet-Visible Absorption Spectrometry
Nuclear Magnetic Resonance Spectrometry
Mass Spectrometry
Qualitative Tests for the Elements
Qualitative Characterization Tests: Tests for Functional Groups
Characterization Through Formation of Derivatives
Assembling the Apparatus
Temperature Control
Methods of Heating and Cooling
Stirring
Addition of Reagents
Control of Evolved Gases
Concentration
Use of an Inert Atmosphere
Working Up the Reaction

Notă biografică

ADDISON AULT is Professor of Chemistry at Cornell College in Mount Vernon, Iowa, where he has taught since 1962.

Caracteristici

1 Explains how to perform experimental procedures and prepare a variety of organic compounds
2 Teaches students the theory behind the techniques as they use them
3 Includes substitutions, additions, eliminations and 'name' reactions as well as procedures for the preparation of interesting compounds such as aspirin and the alarm pheromone of the honey bee

Descriere

Ideally suited for second-year undergraduate organic chemistry laboratory courses, this text explains how to perform operations and prepare a variety of organic compounds. As they learn how to filter a hot solution, recrystallize a solid, distil a liquid, perform an extraction and dry a solution, students will come to understand the theory behind the techniques. The book includes substitutions, additions, eliminations and `name' reactions such as the Grignard reaction and the Wittig synthesis as well as procedures for the preparation of interesting compounds such as aspirin and the alarm pheromone of the honey bee.