Analytical Pyrolysis Handbook
Editat de Karen D. Sam, Thomas P. Wampleren Limba Engleză Paperback – 26 sep 2022
The much-anticipated third edition incorporates recent technological advances that increase the technique’s sensitivity to trace elements, improve its reproducibility, and expand its applicability. The book reviews the types of instrumentation available to perform pyrolysis and offers guidance for interfacing instruments and integrating other analytical techniques, including gas chromatography and mass spectrometry. Fully updated with new sample pyrograms, figures, references, and real-world examples, this edition also highlights new areas of application including cultural materials, forensic analysis, and environmental studies.
This book illustrates how the latest advances make pyrolysis a practical, cost-effective, reliable, and flexible alternative for increasingly complex sample analyses. Analytical Pyrolysis Handbook, Third Edition is an essential, one-stop guide for determining if pyrolysis meets application-specific needs as well as performing pyrolysis and handling the data obtained.
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Specificații
ISBN-13: 9780367740542
ISBN-10: 0367740540
Pagini: 326
Ilustrații: 24 Tables, black and white; 249 Line drawings, black and white; 18 Halftones, black and white; 267 Illustrations, black and white
Dimensiuni: 178 x 254 x 24 mm
Greutate: 0.86 kg
Ediția:3 ed
Editura: CRC Press
Colecția CRC Press
ISBN-10: 0367740540
Pagini: 326
Ilustrații: 24 Tables, black and white; 249 Line drawings, black and white; 18 Halftones, black and white; 267 Illustrations, black and white
Dimensiuni: 178 x 254 x 24 mm
Greutate: 0.86 kg
Ediția:3 ed
Editura: CRC Press
Colecția CRC Press
Public țintă
ProfessionalCuprins
Contents
Preface...............................................................................................................................................ix
Editors ...............................................................................................................................................xi
List of Contributors ........................................................................................................................xiii
Chapter 1 Analytical Pyrolysis: An Overview ............................................................................1
Thomas P. Wampler
Chapter 2 Instrumentation and Analysis....................................................................................23
Thomas P. Wampler
Chapter 3 Pyrolysis Mass Spectrometry:
Instrumentation, Techniques, and Applications ......................................................................39
C. J. Maddock, T. W. Ottley, and Thomas P. Wampler
Chapter 4 Microstructure of Polyolefins....................................................................................55
Shin Tsuge and Hajime Ohtani
Chapter 5 Degradation Mechanisms of Condensation Polymers:
Polyesters and Polyamides........................................................................................69
Hajime Ohtani and Shin Tsuge
Chapter 6 The Application of Analytical Pyrolysis to the Study
of Cultural Materials .................................................................................................89
Chapter 7 Environmental Applications of Pyrolysis ...............................................................115
Thomas O. Munson, Karen D. Sam, and Alexandra ter Halle
Chapter 8 Examination of Forensic Evidence.........................................................................147
John M. Challinor, David A. DeTata, Kari M. Pitts, and Céline Burnier
Chapter 9 Characterization of Microorganisms by Pyrolysis-GC,
Pyrolysis-GC/MS, and Pyrolysis-MS .....................................................................171
Stephen L. Morgan, Bruce E. Watt, and Randolph C. Galipo
Chapter 10 Analytical Pyrolysis of Polar Macromolecules ......................................................197
Charles Zawodny and Karen D. Sam
Chapter 11 Characterization of Condensation Polymers by Thermally
Assisted Hydrolysis and Methylation-GC ..............................................................215
Hajime Ohtani and Shin Tsuge
Chapter 12 Index of Sample Pyrograms.................................................................................235
Karen D. Sam
Index..............................................................................................................................................303
Preface...............................................................................................................................................ix
Editors ...............................................................................................................................................xi
List of Contributors ........................................................................................................................xiii
Chapter 1 Analytical Pyrolysis: An Overview ............................................................................1
Thomas P. Wampler
Chapter 2 Instrumentation and Analysis....................................................................................23
Thomas P. Wampler
Chapter 3 Pyrolysis Mass Spectrometry:
Instrumentation, Techniques, and Applications ......................................................................39
C. J. Maddock, T. W. Ottley, and Thomas P. Wampler
Chapter 4 Microstructure of Polyolefins....................................................................................55
Shin Tsuge and Hajime Ohtani
Chapter 5 Degradation Mechanisms of Condensation Polymers:
Polyesters and Polyamides........................................................................................69
Hajime Ohtani and Shin Tsuge
Chapter 6 The Application of Analytical Pyrolysis to the Study
of Cultural Materials .................................................................................................89
Chapter 7 Environmental Applications of Pyrolysis ...............................................................115
Thomas O. Munson, Karen D. Sam, and Alexandra ter Halle
Chapter 8 Examination of Forensic Evidence.........................................................................147
John M. Challinor, David A. DeTata, Kari M. Pitts, and Céline Burnier
Chapter 9 Characterization of Microorganisms by Pyrolysis-GC,
Pyrolysis-GC/MS, and Pyrolysis-MS .....................................................................171
Stephen L. Morgan, Bruce E. Watt, and Randolph C. Galipo
Chapter 10 Analytical Pyrolysis of Polar Macromolecules ......................................................197
Charles Zawodny and Karen D. Sam
Chapter 11 Characterization of Condensation Polymers by Thermally
Assisted Hydrolysis and Methylation-GC ..............................................................215
Hajime Ohtani and Shin Tsuge
Chapter 12 Index of Sample Pyrograms.................................................................................235
Karen D. Sam
Index..............................................................................................................................................303
Notă biografică
Karen D. Sam is an Application Scientist and Lab Manager at CDS Analytical. She has over 20 years of
experience in sample preparation and analysis, including 15 years in application development
experience, supporting the design and testing of analytical pyrolysis instruments. She is the author
or co-author of several professional papers on the use of analytical pyrolysis. She holds an A.A.
degree from Cottey College in Nevada, MO, and a B.S. degree in Chemistry from Bloomsburg
University, in Bloomsburg, Pennsylvania.
Thomas P. Wampler earned his B.S. degree (1970) in chemistry and an M.Ed. degree (1973) in
natural science from the University of Delaware in Newark, Delaware. Currently retired, he was
actively engaged in the field of analytical pyrolysis for over 25 years. He was the director of
science and technology at CDS Analytical, LLC, in Oxford, Pennsylvania. He is the author and
coauthor of numerous professional papers on the use of analytical pyrolysis and other thermal
sampling techniques.
experience in sample preparation and analysis, including 15 years in application development
experience, supporting the design and testing of analytical pyrolysis instruments. She is the author
or co-author of several professional papers on the use of analytical pyrolysis. She holds an A.A.
degree from Cottey College in Nevada, MO, and a B.S. degree in Chemistry from Bloomsburg
University, in Bloomsburg, Pennsylvania.
Thomas P. Wampler earned his B.S. degree (1970) in chemistry and an M.Ed. degree (1973) in
natural science from the University of Delaware in Newark, Delaware. Currently retired, he was
actively engaged in the field of analytical pyrolysis for over 25 years. He was the director of
science and technology at CDS Analytical, LLC, in Oxford, Pennsylvania. He is the author and
coauthor of numerous professional papers on the use of analytical pyrolysis and other thermal
sampling techniques.
Descriere
Provides a comprehensive view of analytical pyrolysis, beginning with theory and instrumentation, and a vast view of current applications. Provides readers with an essential, one-stop guide for determining if pyrolysis meets application-specific needs, performing pyrolysis, and handling data.