Microwave-assisted Organic Synthesis: One Hundred Reaction Procedures: Tetrahedron Organic Chemistry, cartea 25
Autor D. Bogdalen Limba Engleză Hardback – 2 dec 2005
- Provides a broad overview of microwave enhanced chemistry
- Written by internationally renowned scientists
- Includes exercises and worked problems which can support more independent study
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Specificații
ISBN-13: 9780080446219
ISBN-10: 0080446213
Pagini: 214
Ilustrații: 1
Dimensiuni: 165 x 240 x 13 mm
Greutate: 0.53 kg
Editura: ELSEVIER SCIENCE
Seria Tetrahedron Organic Chemistry
ISBN-10: 0080446213
Pagini: 214
Ilustrații: 1
Dimensiuni: 165 x 240 x 13 mm
Greutate: 0.53 kg
Editura: ELSEVIER SCIENCE
Seria Tetrahedron Organic Chemistry
Public țintă
Advanced undergraduate and graduate students and researchers or lecturers in Organic chemistryCuprins
1. Preface
2. Interaction of microwaves with different materials
3. Microwave effect vs. thermal effect
3.1. Thermal activation during microwave irradiation
3.2. Non-thermal activation during microwave irradiation
4. Microwave equipment
4.1. Microwave generators
4.2. Transmission lines (waveguides)
4.3. Microwave applicators (cavities)
4.4. Microwave reactors
4.5. Temperature monitoring
4.6. Reaction vessels and glassware
5. Techniques for conducting chemical reactions under microwave irradiation
6. Safety precautions on the application of microwaves in laboratory
7. Reactions under microwave conditions
7.1. Reactions in homogenous media
7.2. Reactions of reagents supported on mineral supports
7.3. Solid-liquid solvent-free phase transfer catalysis (PTC) reactions
7.4. Reactions of neat reagents
7.5. Polymerization reactions
8. Concluding remarks
2. Interaction of microwaves with different materials
3. Microwave effect vs. thermal effect
3.1. Thermal activation during microwave irradiation
3.2. Non-thermal activation during microwave irradiation
4. Microwave equipment
4.1. Microwave generators
4.2. Transmission lines (waveguides)
4.3. Microwave applicators (cavities)
4.4. Microwave reactors
4.5. Temperature monitoring
4.6. Reaction vessels and glassware
5. Techniques for conducting chemical reactions under microwave irradiation
6. Safety precautions on the application of microwaves in laboratory
7. Reactions under microwave conditions
7.1. Reactions in homogenous media
7.2. Reactions of reagents supported on mineral supports
7.3. Solid-liquid solvent-free phase transfer catalysis (PTC) reactions
7.4. Reactions of neat reagents
7.5. Polymerization reactions
8. Concluding remarks
Recenzii
"Bogdal's book is more of a practical guide to using the techniques of microwave-assisted organic synthesis in the laboratory. The book is well suited for both undergraduate and beginning graduate students. The 87 tested experimental procedures truly set this work apart from previous books on the subject. Summing Up: Highly recommended. Lower-division undergraduates through professionals; two-year technical program students." --CHOICE, September 2006, L.J. Liotta, Stonehill College