Organic Syntheses, Volume 97 (Organic Syntheses) de M Movassaghi

Organic Syntheses, Volume 97: Organic Syntheses

M Movassaghi

The current volume continues the tradition of the Organic Syntheses series, providing carefully checked and edited experimental procedures that describe important synthetic methods, transformations, reagents, and synthetic building blocks or intermediates with demonstrated utility in organic synthesis. These significant and interesting procedures should prove worthwhile to many synthetic chemists working in increasingly diverse areas. A trusted guide for professionals in organic and medicinal chemistry in academia, government, and industries, including pharmaceuticals, fine chemicals, agrochemicals, and biotechnological products.

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Cuprins

Discussion Addendum for: Synthesis of Arylboronic Pinacol Esters from Corresponding Arylamines 1 Fanyang Mo, Di Qiu, and Jianbo Wang Deaminative Functionalization of Primary Sulfonamides 12 Patrick S. Fier and Kevin M. Maloney Synthesis of 3,6-Bis(dimethylamino)-9H-xanthen-9-one by Stepwise Chemical Redox Cycling 21 James L. Bachman, Cyprian I. Pavlich, and Eric V.Anslyn Preparation of (-)-Levoglucosenone from Cellulose Using Sulfuric Acid in Polyethylene Glycol 38 J. Klepp, W. Dillon, Y. Lin, P. Feng, and B. W. Greatrex Scalable Preparation of O-(Diphenylphosphinyl) hydroxylamine (DPPH) 54 Tamas Benkovics, Andrew J. Neel, Ralph Zhao, and Gregory J. Hughes Discussion Addendum for: Dibenzo[a,e]cyclooctene: Multigram Synthesis of a Bidentate Ligand 66 Günter Helmchen Discussion Addendum for: (S)-(-)-2-Allylcyclohexanone (2-Allylcyclohexan-1-one] 79 Manfred Braun Synthesis of 4-Nitrophenyl (2,2,6,6-Tetramethylpiperidin-1-yl) Carbonate (NPTC) for N-Protection of L-Phenylalanine Ethyl Ester 96 Joseph R. Lizza and Peter Wipf Discussion Addendum for: Pd-Catalyzed External-CO-Free Carbonylation: Preparation of 2,4,6-Trichlorophenyl 3,4-Dihydronaphthalene-2-Carboxylate 125 Hideyuki Konishi and Kei Manabe From 5-Hydroxynicotinic Acid to Nitrogenous (4+3)-Cycloadducts 139 Alexander S. Harmata and Michael Harmata Synthesis of alpha-Bromoacetyl MIDA Boronate 157 C. Frank Lee, Chieh-Hung Tien, Shinya Adachi, and Andrei K. Yudin Synthesis of Chiral Bisoxazoline Ligands: (3aR,3a'R,8aS,8a'S)-2,2'- (cyclopropane-1,1-diyl)bis(3a,8a-dihydro-8H-indeno[1,2-d]oxazole) 172 Julie L. Hofstra, Travis J. DeLano, and Sarah E. Reisman Synthesis of 2,5-Diaryloxadiazinones 189 Andrew V. Kelleghan, Katie A. Spence, and Neil K. Garg Preparation of O-Pivaloyl Hydroxylamine Triflic Acid 207 Szabolcs Makai, Eric Falk, and Bill Morandi Preparation of a Z-Iodoalkene through Stork-Zhao-Wittig Olefination, Stereo-retentive Lithium-iodine Exchange and Z-Boronic acid Pinaco Ester Synthesis 217 Mathieu A. Morin, Samantha Rohe, Cecile Elgindy, and Michael S. Sherburn Discussion Addendum for: Synthesis of Substituted Indazoles via [3 + 2] Cycloaddition of Benzyne and Diazo Compounds 232 Anton V. Dubrovskiy and Richard C. Larock Anhydrous, Homogeneous, Suzuki-Miyaura Cross-Coupling of Boronic Esters using Potassium Trimethylsilanolate 245 Connor P. Delaney, Ethan M. Heyboer, and Scott E. Denmark Stereoselective Synthesis of Chiral Sulfinamide Monophosphine Ligands (Ming-Phos)(S, Rs)-M 262 Anjing Hu, Zhan-Ming Zhang, Yuanjing Xiao, and Junliang Zhang Preparation of Asymmetric Phase-transfer Catalyst, 1,4-Bis((4S,5S)- 1,3-bis(3,5-di-tert-butylbenzyl)-4,5-diphenylimidazolidin-2-ylidene)piperazine-1,4-diium chloride 274 Esther Cai Xia Ang, Xinyi Ye, and Choon-Hong Tan Oxidation of Aldehydes to Nitriles with an Oxoammonium Salt: Preparation of Piperonylonitrile 294 Nathaniel D. Kaetzel, Kyle M. Lambert, and Christopher B. Kelly Preparation of 1H-Indazole-3-carbonitrile 314 Yonggang Chen, Qinghao Chen, Lushi Tan, Lu Chen, and Xiaowei Wang Asymmetric Michael Addition of Dimethyl Malonate to 2-Cyclopenten-1-one Catalyzed by a Heterobimetallic Complex 327 Nicholas J. Fastuca, Alice R. Wong, Victor W. Mak, and Sarah E. Reisman Discussion Addendum for: Synthesis of Et2SBr*SbCl5Br and its Use in Biomimetic Brominative Polyene Cyclizations 339 Cooper A. Taylor and Scott A. Snyder Nickel-Catalyzed Arylboration of Cyclopentene 355 Stephen R. Sardini and M. Kevin Brown