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XAFS for Everyone

Autor Scott Calvin
en Limba Engleză Paperback – 20 mai 2013
XAFS for Everyone provides a practical, thorough guide to x-ray absorption fine-structure (XAFS) spectroscopy for both novices and seasoned practitioners from a range of disciplines. The text is enhanced with more than 200 figures as well as cartoon characters who offer informative commentary on the different approaches used in XAFS spectroscopy.
The book covers sample preparation, data reduction, tips and tricks for data collection, fingerprinting, linear combination analysis, principal component analysis, and modeling using theoretical standards. It describes both near-edge (XANES) and extended (EXAFS) applications in detail. Examples throughout the text are drawn from diverse areas, including materials science, environmental science, structural biology, catalysis, nanoscience, chemistry, art, and archaeology. In addition, five case studies from the literature demonstrate the use of XAFS principles and analysis in practice. The text includes derivations and sample calculations to foster a deeper comprehension of the results.
Whether you are encountering this technique for the first time or looking to hone your craft, this innovative and engaging book gives you insight on implementing XAFS spectroscopy and interpreting XAFS experiments and results. It helps you understand real-world trade-offs and the reasons behind common rules of thumb.
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Specificații

ISBN-13: 9781439878637
ISBN-10: 1439878633
Pagini: 460
Ilustrații: 325 black & white illustrations, 9 colour illustrations, 18 black & white tables
Dimensiuni: 210 x 280 x 23 mm
Greutate: 1.08 kg
Ediția:New.
Editura: CRC Press
Colecția CRC Press

Public țintă

Postgraduate and Undergraduate

Notă biografică

Scott Calvin is the chair of the Division of Natural Science and Mathematics at Sarah Lawrence College, where he teaches innovative courses, including crazy ideas in physics, rocket science, and steampunk physics. He is also a member of the principal research team for beamline X-11B at the National Synchrotron Light Source. Since 1998, he has been using XAFS to study systems as diverse as solar cells, magnetic nanoparticles, soil samples, battery cathodes, analogues to atmospheric dust particles, and pigments used in 18th century painting. He received a PhD in physics from Hunter College of the City University of New York.

Cuprins

The XAFS Experiment: XAFS in a Nutshell. Planning the Experiment. Sample Preparation. Data Reduction. Data Collection. XAFS Analysis: Fingerprinting. Linear Combination Analysis. Principle Component Analysis. Curve Fitting to Theoretical Standards. Modeling: A Dictionary of Parameters. Identifying a Good Fit. The Process of Fitting. Starting Structures. Constraints. XAFS in the Literature: Communicating XAFS. Case Studies. Appendix. Index.

Recenzii

"The book is very timely … It is unique in covering theoretical background and experimental details to data analysis in a way that is easy to understand. It will be very valuable to anyone who is interested in using x-ray spectroscopy by helping them to better design and get more out of their experiments."
—Dr. Chi-Chang Kao, Director, SLAC National Accelerator Laboratory
"The author has found fun and engaging ways to explain details of XAFS that otherwise can seem so dry. I am sure that folks who use my beamline and software will love XAFS for Everyone."
—Dr. Bruce Ravel, National Institute of Standards and Technology
"A unique presentation with great value for readers and special emphasis on practical aspects … a ‘must have’ for XAFS scientists and beamlines."
—Prof. Mark C. Ridgway, Department of Electronic Materials Engineering, Australian National University
"This book will be useful to graduate students, post docs, and researchers. I highly recommend it."
—Dr. Richard W. Strange, Molecular Biophysics, The University of Liverpool

Descriere

This text provides a practical, thorough guide to x-ray absorption fine-structure (XAFS) spectroscopy for both novices and seasoned practitioners from a range of disciplines. Cartoon characters and easy-to-follow illustrations introduce multiple viewpoints without distracting from the main narrative. Whether you are encountering this technique for the first time or looking to hone your craft, this innovative and engaging book gives you insight on implementing XAFS spectroscopy and interpreting XAFS experiments and results. It helps you understand real-world trade-offs and the reasons behind common rules of thumb.