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High Vacuum Techniques for Chemical Syntheses and Measurements

Autor P. H. Plesch
en Limba Engleză Paperback – 14 dec 2005
This 1989 book describes the physico-chemical principles of the high vacuum techniques used by chemists. It is a guide to the choice of suitable equipment, the methods of constructing the systems, and the ways of using them. Professor Plesch's book is the only up-to-date work on the type of high vacuum systems (HVS) used by chemists and it is the first ever to describe in detail the actual construction, manifold uses, method of operation, and final dismantling of an HVS. It includes descriptions of a very wide range of devices for making measurements (conductivity, spectra, kinetics, etc.) in vacuum. The author draws on over 40 years of his own experiences and those of others in many parts of the world, and many of the tricks and gadgets have not been published before. The book will be an essential companion on the bench of every chemist involved in the synthesis of, or measurements on, air-sensitive compounds.
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Specificații

ISBN-13: 9780521675475
ISBN-10: 0521675472
Pagini: 184
Ilustrații: 63 b/w illus. 8 tables
Dimensiuni: 157 x 234 x 10 mm
Greutate: 0.27 kg
Ediția:Revised
Editura: Cambridge University Press
Colecția Cambridge University Press
Locul publicării:Cambridge, United Kingdom

Cuprins

1. Fundamentals; 2. The main vacuum line; 3. Appliances and procedures; 4. Purification, including drying; 5. Doing chemistry with high vacuum systems.

Recenzii

' … a very useful addition to the bookshelf and one which, by advocating simplicity of operation, will give the reader confidence to use high vacuum systems in dealing with air-sensitive compounds …' Chemistry in Britain
' … an essential companion on the bench of every chemist …' Laboratory News

Descriere

This 1989 book describes the principles and techniques of isolating air-sensitive chemicals from the atmosphere.