Polymer Synthesis and Characterization: A Laboratory Manual
Autor Stanley R. Sandler, Wolf Karo, JoAnne Bonesteel, Eli M. Pearceen Limba Engleză Paperback – 20 mai 1998
- Combines the extensive industrial and teaching experience of the authors
- Introduces the user to the concept of "Good Manufacturing Practice"
- Presents experiments that are representative of a wide variety of polymerization and characterization methods
- Includes numerous references for more advanced students, technicians, and researcher
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Specificații
ISBN-13: 9780126182408
ISBN-10: 012618240X
Pagini: 232
Dimensiuni: 229 x 152 x 19 mm
Greutate: 0.65 kg
Editura: ELSEVIER SCIENCE
ISBN-10: 012618240X
Pagini: 232
Dimensiuni: 229 x 152 x 19 mm
Greutate: 0.65 kg
Editura: ELSEVIER SCIENCE
Public țintă
Audience: Upper division undergraduate and first year graduate students in polymer chemistry, as well as industrial chemists individually or involved in corporate training. Students will be enrolled in both chemistry and materials science departments.Cuprins
Polymer
Syntheses:A.
Polymerization
of
Styrene:Experiment
1:
Preparation
of
Polystyrene
by
the
Free
Radical
Polymerization
Process.
Experiment
2:
Preparation
of
Polystyrene
by
the
Emulsion
Polymerization
Process.
Experiment
3:
Preparation
of
Polystyrene
by
the
Anionic
Polymerization
Method.
Experiment
4:
Preparation
of
Polystyrene
by
the
Cationic
Polymerization
Process.B.
Polymerization
of
Acrylic
Esters:Experiment
5:
Bulk
Photopolymerization
of
Methyl
Methacrylate:
A
Test
Tube
Demonstration.
Experiment
6:
Suspension
Polymerization
of
Methyl
Methacrylate.
Experiment
7:
Redox
Emulsion
Polymerization
of
Ethyl
Acrylate.C.
Polyamides:Experiment
8:
Preparation
of
Poly(hexamethylene
sebacamide)(Nylon
6-10)
by
the
Interfacial
Polymerization
Technique.D.
Polyesters:Experiment
9:
Preparation
of
Poly(1,4-butylene
isophthalate).E.
Epoxy
Resins:Experiment
10:
Preparation
of
A
Cured
Epoxy
Resin
by
the
Room
Temperature
Reaction
ofBisphenol
A
Diglycidyl
Ether
with
Polyamines.F.
Vinyl
Acetate
Polymers
and
Reactions:Experiment
11:
Seed
Emulsion
Terpolymerization
of
Vinyl
Acetate,
Butyl
Acrylate,
and
Vinyl
Neodecanoate
with
Gradual
Monomer
and
Initiator
Additions.
Experiment
12:
Preparation
of
Poly(vinyl
alcohol)
by
the
Alcoholysis
of
Poly(vinyl
Acetate).Polymer
Characterization:Experiment
13:
Nuclear
Magnetic
Resonance.
Experiment
14:
Infrared
Spectroscopy.
Experiment
15:
Thermogravimetric
Analysis.
Experiment
16:Differential
Scanning
Calorimetry.
Experiment
17:
Dilute
Solution
Viscosity
of
Polymers.
Experiment
18:
Gel
Permeation
Chromatography.
Experiment
19:
Light
Scattering.
Experiment
20:
End
Group
Analysis.
Experiment
21:
X-Ray
Diffraction.
Experiment
22:
Optical
Microscopy.
Experiment
23:
Dynamic
Mechanical
Analysis.
Subject
Index.
Recenzii
"...recommended
for
organizers
of
practical
courses
in
polymer
chemistry
and
for
the
students
taking
part
in
these
courses.
It
provides
useful
advice
on
planning
and
managing
appropriate
experiments,
and
gives
a
comprehensive
introduction
to
important
techniques
for
polymer
synthesis
and
characterization.
A
very
positive
feature
is
the
clear
writing
style
and
the
straightforward
approach
to
concepts
and
procedures."
--ANGEWANDTE
CHEMIE,
Vol.
38,
No.
18,
1999