Quantitation of Amino Acids and Amines by Chromatography: Methods and Protocols: Journal of Chromatography Library, cartea 70
Editat de Ibolya Molnár-Perlen Limba Engleză Hardback – 27 iun 2005
The characteristics of the given chromatographic procedure, relating to the topic in question, are classified according to the preliminary preparation/derivatization process(es), which means the simple methods, suitable for the analysis of the selected compound(s) in natural form, are followed by various derivatization proposals. Detailed protocols provide the reader with guidance in beginning tasks and on how to improve current methods. This book appeals to a wide audience and is recommended for those looking towards the wider reaches of identification and quantification of amino acids and amines.
- Provides a systematic, and comprehensive summary of chromatographic techniques and derivatization processes
- Compares advantages/disadvantages of various chromatographic techniques
- Readers can undertake practical tasks using detailed protocols given in the book
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Specificații
ISBN-13: 9780444520500
ISBN-10: 0444520503
Pagini: 668
Dimensiuni: 165 x 240 x 30 mm
Greutate: 1.38 kg
Editura: ELSEVIER SCIENCE
Seria Journal of Chromatography Library
ISBN-10: 0444520503
Pagini: 668
Dimensiuni: 165 x 240 x 30 mm
Greutate: 1.38 kg
Editura: ELSEVIER SCIENCE
Seria Journal of Chromatography Library
Public țintă
Students and post graduates, researchers in universities in academia and research Laboratories; Practitioners and consultants in environmental testing laboratories and the food and pharmaceutical industryCuprins
Part 1. Amino Acids
1.1. Gas Chromatography
1.1.1. Quantitation of Amino Acids as Chloroformates - A Return to Gas Chromatography (P. Hu&sbreve;ek).
1.1.2. Quantitation of Amino Acids by Gas-Liquid Chromatography (C.W. Gehrke).
1.1.3. Chiral separations of Amino Acids by Gas Chromatography (R. Pätzold, H. Brückner).
1.2. High Performance Liquid Chromatography
1.2.1. HPLC of Amino Acids without Derivatization (C. Elfakir).
1.2.2. HPLC of Amino Acids as Phenylthiocarbamoyl Derivatives (I. Molnár-Perl).
1.2.3. HPLC of Amino Acids as o-Phthalaldehyde Derivatives (I. Molnár-Perl).
1.2.4. HPLC of Amino Acids as Chloroformate Derivatives (B. Josefsson).
1.2.5. HPLC of Amino Acids as Dansyl and Dabsyl Derivatives (Toyohide Takeuchi).
1.2.6. Quantitation of Amino Acids as 6-Aminoquinolyl-N-hydroxysuccinimidyl Carbamate Derivatives (S.A. Cohen).
1.3. Capillary Electrophoresis/Capillary Electrochromatography
1.3.1. Determination of Underivatized Amino Acids by Capillary Electrophoresis and Capillary Electrochromatography (C.W. Klampfl).
1.3.2. Quantitation of Amino Acids as o-Phthalaldehyde derivatives (Shigeyuki Oguri).
1.3.3 Capillary Electrophoresis and Capillary Electrochromatography of Amino Acids as Dansyl Derivatives (Zilin Chen).Part 2. Amines
2.1. Gas Chromatography
2.1.1. Gas Chromatographic Determination of Volatile Aliphatic and Selected Aromatic Amines, without Derivatization: Solid Phase Microextraction (J. Namiesnik, B. Zigmunt).
2.1.2. Gas Chromatography of Amines as Various Derivatives (Hiroyuki Kataoka).
2.2. High Performance Liquid Chromatography
2.2.1. HPLC of Amines as o-Phthalaldehyde Derivatives (I. Molnár-Perl).
2.2.2. Quantitation by HPLC of Amino Acids as Dansyl Derivatives (M. Silva).
2.2.3. HPLC of Amines as 9-Fluorenylmethyl Chloroformate Derivatives (Paul Chi Ho).
2.2.4. HPLC of Biogenic Amines as 6-Aminoquinolyl-N-hydroxysuccinimidyl Derivatives (T.S. Weiss).
2.3. Capillary Electrophoresis/Capillary Electrochromatography
2.3.1. Determination of Underivatized Amines by CE and CEC (C.W. Klampfl).
2.3.2. Quantitation of Amines by Oncolumn Derivatives with o-Phthalaldehyde by CEC (Shigeyuki Oguri).
3. Quantitation of Amino Acids and Amines, Simultaneously (I. Molnár-Perl).
4. Quantitation of Polyamines by Chromatography (Y. Mengerink).
1.1. Gas Chromatography
1.1.1. Quantitation of Amino Acids as Chloroformates - A Return to Gas Chromatography (P. Hu&sbreve;ek).
1.1.2. Quantitation of Amino Acids by Gas-Liquid Chromatography (C.W. Gehrke).
1.1.3. Chiral separations of Amino Acids by Gas Chromatography (R. Pätzold, H. Brückner).
1.2. High Performance Liquid Chromatography
1.2.1. HPLC of Amino Acids without Derivatization (C. Elfakir).
1.2.2. HPLC of Amino Acids as Phenylthiocarbamoyl Derivatives (I. Molnár-Perl).
1.2.3. HPLC of Amino Acids as o-Phthalaldehyde Derivatives (I. Molnár-Perl).
1.2.4. HPLC of Amino Acids as Chloroformate Derivatives (B. Josefsson).
1.2.5. HPLC of Amino Acids as Dansyl and Dabsyl Derivatives (Toyohide Takeuchi).
1.2.6. Quantitation of Amino Acids as 6-Aminoquinolyl-N-hydroxysuccinimidyl Carbamate Derivatives (S.A. Cohen).
1.3. Capillary Electrophoresis/Capillary Electrochromatography
1.3.1. Determination of Underivatized Amino Acids by Capillary Electrophoresis and Capillary Electrochromatography (C.W. Klampfl).
1.3.2. Quantitation of Amino Acids as o-Phthalaldehyde derivatives (Shigeyuki Oguri).
1.3.3 Capillary Electrophoresis and Capillary Electrochromatography of Amino Acids as Dansyl Derivatives (Zilin Chen).Part 2. Amines
2.1. Gas Chromatography
2.1.1. Gas Chromatographic Determination of Volatile Aliphatic and Selected Aromatic Amines, without Derivatization: Solid Phase Microextraction (J. Namiesnik, B. Zigmunt).
2.1.2. Gas Chromatography of Amines as Various Derivatives (Hiroyuki Kataoka).
2.2. High Performance Liquid Chromatography
2.2.1. HPLC of Amines as o-Phthalaldehyde Derivatives (I. Molnár-Perl).
2.2.2. Quantitation by HPLC of Amino Acids as Dansyl Derivatives (M. Silva).
2.2.3. HPLC of Amines as 9-Fluorenylmethyl Chloroformate Derivatives (Paul Chi Ho).
2.2.4. HPLC of Biogenic Amines as 6-Aminoquinolyl-N-hydroxysuccinimidyl Derivatives (T.S. Weiss).
2.3. Capillary Electrophoresis/Capillary Electrochromatography
2.3.1. Determination of Underivatized Amines by CE and CEC (C.W. Klampfl).
2.3.2. Quantitation of Amines by Oncolumn Derivatives with o-Phthalaldehyde by CEC (Shigeyuki Oguri).
3. Quantitation of Amino Acids and Amines, Simultaneously (I. Molnár-Perl).
4. Quantitation of Polyamines by Chromatography (Y. Mengerink).